Thermal Analysis
Mostrando 1-12 de 1892 artigos, teses e dissertações.
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1. Catalysts Derived from Thermal Treatments of Hydrocalumite-Type Compounds: Synthesis and Application in Transesterification Reactions
Catalyst performance is a relevant factor in biodiesel production because it can affect the efficiency of the process. This work provides a study of the performance of heterogeneous catalysts for biodiesel production derived from thermal-treated hydrocalumite-type compounds. This work aimed to synthesize and characterize hydrocalumite-type compounds intercal
Journal of the Brazilian Chemical Society. Publicado em: 2023
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2. Tailoring the properties of Y2O3 via synthesis parameters varied during the PVA-assisted sol-gel route
Abstract The effect of synthesis parameters on the microstructural behavior and morphology during the yttrium oxide (Y2O3) formation is reported. Y2O3 crystals were produced by a modified sol-gel route assisted by polyvinyl alcohol solution varying the calcination temperature and solution pH. The crystalline phase formation was investigated using X-ray powde
Cerâmica. Publicado em: 2023
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3. Bioactive SiO2-K2O-CaO-P2O5 glass-ceramic scaffold prepared using polyurethane foam template
Abstract A glass-ceramic in the SiO2-K2O-CaO-P2O5 quaternary system was prepared by substituting the Na2O component with K2O to avoid Na2Ca2Si3O9 formation upon thermal treatment since this phase decreases apatite formation kinetics on glass material. To form the glass-ceramic, a modified sol-gel method involving solution precipitation, followed by reagents
Cerâmica. Publicado em: 2023
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4. Study of nanocomposites with carbon nanotubes and their tendency for carbon organization
Abstract The carbon derived from the thermal treatment of modified phenolic resins (PR) tends to organize into graphitic lamellae or turbostratic carbon and is commonly considered non-graphitizable. In this study, nanocomposites were synthesized with modified phenolic resin (Novolac) used as the matrix and oxidized multi-walled carbon nanotubes (NTox) in amo
Cerâmica. Publicado em: 2022
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5. Reliability of quantitative sensory testing on myofascial trigger points in the upper trapezius muscle of individuals with chronic neck pain
SUMMARY OBJECTIVE: The objective of this study was to measure the intra- and inter-rater reliability of the quantitative sensory testing for measuring the thermal pain threshold on myofascial trigger points in the upper trapezius muscle of individuals with chronic neck pain. METHODS: Thirty female participants were included, aged between 18 and 45 years an
Revista da Associação Médica Brasileira. Publicado em: 2022
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6. Finite element computational development for thermo-mechanical analysis of plane steel structures exposed to fire
Abstract This article presents a numerical formulation based on finite element procedures for application in nonlinear thermo-mechanical analyses of steel planar structures under fire condition. The mechanical properties of structural elements degrade when subjected to high temperatures, resulting in significant reductions in strength and stiffness. Under th
REM - International Engineering Journal. Publicado em: 2022
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7. Quality Control for Lignin and Gelatin Microcapsules Loaded with Orange Essential Oil
Sustainable natural product-based microstructured systems and biopolymers are strong candidates for use in crop protection. Lignin and gelatin microcapsules loaded with orange essential oil were developed with spray-drying in order to enhance its potential. We evaluated the microparticle controlled release mechanisms, biological effects, structural and therm
Journal of the Brazilian Chemical Society. Publicado em: 2022
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8. Post-Occupancy Evaluation of an educational building: Case study of the ETS-UESC Building
Abstract The physical and environmental conditions of educational institutions are determining factors for occupant comfort. The Post-Occupancy Evaluation (POE) presents itself as a methodology for verifying environmental aspects in full use, considering the technical criteria and the users' perception. This article discusses the particularities of the ETS-U
REM - International Engineering Journal. Publicado em: 2022
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9. Catalytic Effects of Ruthenocene Bimetallic Compounds Derived from Fused Aromatic Ring Ligands on the Main Oxidizing Agent for Solid Rocket Motor
We report the catalytic effect of three ruthenocene bimetallic compounds derived from fused aromatic rings of general formula [{Cp*Ru}2L], with Cp*: pentamethylcyclopentadiene and L = pentalene (1), 2,6-diethyl-4,8-dimethyl-s-indacene (2), and 2,7-diethyl-as-indacene (3), on the thermal decomposition of ammonium perchlorate (AP). The new compound 3 was chara
Journal of the Brazilian Chemical Society. Publicado em: 2022
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10. K2O SUPORTADO EM ZEÓLITA NATURAL: SÍNTESE, CARACTERIZAÇÃO E APLICAÇÃO PRODUÇÃO DE BIODIESEL A PARTIR DO ÓLEO DE GIRASSOL
Biodiesel is a renewable fuel, a substitute for fossil diesel, which is important for reducing GHG in Brazil. Therefore, this work aims to synthesize and characterize the catalyst using the support of natural zeolite impregnated with K2O and apply it in the production of biodiesel through the transesterification reaction. Through the analysis of characteriza
Química Nova. Publicado em: 2022
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11. Thermal treatment of poultry litter: Part I. Characterization by immediate analysis and gravimetric yield
RESUMO A produção de biocarvão a partir de cama de aviário por meio de pirólise lenta é uma abordagem de valor agregado baseada na fazenda para reciclar o resíduo orgânico. Os experimentos foram conduzidos para examinar como os tratamentos térmicos afetaram a composição final do material carbonizado e pirolisado em relação à análise imediata e
Revista Brasileira de Engenharia Agrícola e Ambiental. Publicado em: 2022
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12. BIODEGRADABLE SODIUM CARBOXYMETHYL CELLULOSE MEMBRANES CONTAINING MELALEUCA ESSENTIAL OILS FOR WOUND CARE MATERIAL
NaCMC is a biocompatible polymer that can be crosslinked with citric acid to form a gel matrix. Melaleuca oils have antimicrobial and anti-inflammatory properties with potential for wound healing. The goal of this work was to investigate the characteristics of NaCMC-Melaleuca oils gels. The gels were characterized by FTIR, TGA, mechanical analysis, and in vi
Química Nova. Publicado em: 2022