Hydrothermal Synthesis
Mostrando 1-12 de 76 artigos, teses e dissertações.
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1. Synthesis and characterization of α-SnWO4 powders obtained by microwave-assisted hydrothermal method
Abstract The structural, morphological, and optical properties of α-SnWO4 synthesized by microwave-assisted hydrothermal method at 150 °C for different times were investigated. XRD revealed the formation of the orthorhombic phase, without the presence of a secondary phase. The sample processed for 64 min showed a reduction in unit cell volume, suggesting a
Cerâmica. Publicado em: 2022
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2. Spectrofluorimetric Determination of Hydrochlorothiazide by a Carbon Dots-Based Probe via Inner Filtering Effect and Resonance Rayleigh Scattering
Synthesis of carbon dots (CDs) from natural resources not only enables green synthesis and production of environmentally friendly materials, but also provides a cost-effective probe as a fluorescence nanosensor. The proposed sensor introduces a unique one-pot hydrothermal CDs synthesis from alfalfa leaves, which is promising for sensing hydrochlorothiazide (
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Phase transformation of kaolinite to hexagonal kalsilite using K2CO3
Abstract Hydrothermal synthesis of kalsilite was facilitated by the inclusion of potassium carbonate (K2CO3) as the source of the potassium ion. After a 24 h reaction at 220 °C, kaolin clay treated with 1.25 M K2CO3 showed the most significant peaks at 2θ of 28.5° and 34.7° by X-ray diffraction corresponding to the hexagonal kalsilite. In addition, field
Cerâmica. Publicado em: 2022
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4. Photoluminescent Investigation of the Doping Site of Eu3+-Doped [Zn3(BTC)2·12H2O] Metal-Organic Framework Prepared by Microwave-Assisted Hydrothermal Synthesis
The [Zn3(BTC)2·12H2O] (BTC = 1,3,5-tricarboxylate) metal-organic framework (MOF) was successfully synthesized using a microwave-assisted hydrothermal synthesis technique, which allowed for significantly decreased reaction time compared to the production of the same compound via conventional heating. In situ doping with Eu3+ ions at concentrations ranging fr
J. Braz. Chem. Soc.. Publicado em: 2020-11
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5. Synthesis and characterization of mesoporous materials with SBA and MCM structure types
Resumo Materiais mesoporosos são estruturas promissoras para aplicação em catálise e adsorção devido à elevada área superficial e grande tamanho dos poros. Materiais mesoporosos foram sintetizados pelo método hidrotérmico com novos surfactantes, distintos daqueles observados na literatura, a fim de realizar um estudo de sua estrutura e obter materi
Cerâmica. Publicado em: 14/11/2019
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6. SYNTHESIS OF MESOPOROUS γ-ALUMINA AND ITS CATALYTIC PERFORMANCE IN DICHLOROPROPANOL CYCLIZATION
This paper discusses the synthesis and resulting catalytic performance of mesoporous alumina using aluminum isopropoxide as the aluminum source, and synthesized organosiloxane KH560-540 as template. The effects of the hydrothermal conditions, as well as the amount of templating agent at pH values of 5-9 on the structure of the synthesized mesoporous alumina
Quím. Nova. Publicado em: 21/10/2019
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7. A FAIR COMPARISON BETWEEN BISMUTH CATALYSTS FOR APPLICATION IN PHOTODEGRADATION UNDER VISIBLE AND SOLAR LIGHT
ABSTRACT Three different bismuth catalysts (Bi2WO6, BiOI and BiVO4) were synthesized using solvo- and hydrothermal methods. Different reaction times, calcination and the addition of poly (vinyl pyrrolidone) during synthesis were tested to investigate the effect of these variables on the catalysts’ morphology and photocatalytic activity. The photocatalytic
Braz. J. Chem. Eng.. Publicado em: 15/07/2019
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8. Hydrothermal Synthesis to Water-stable Luminescent Carbon Dots from Acerola Fruit for Photoluminescent Composites Preparation and its Application as Sensors
Carbon dots (C-dots) possess the attractive properties of high stability, low toxicity, good water solubility, simple synthetic routes as well as size and excitation-dependent photoluminescence (PL).The aim of this work was to synthesize photoluminescent C-dots by hydrothermal method using acerola fruit (Malpighiaemarginata) as a row material, since this fru
Mat. Res.. Publicado em: 06/06/2019
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9. New Synthesis Method for a Core-Shell Composite Based on α-Bi2O3 @PPy and its Electrochemical Behavior as Supercapacitor Electrode
New composite based on polypyrrole (PPy) and bismuth oxide (α-Bi2O3) was investigated as supercapacitor electrode. The α-Bi2O3 was obtained by hydrothermal route at 500 ºC for 2 h. Cyclic voltammetry was used to electropolymerize PPy on graphite electrode (GE) or on GE/α-Bi2O3. The X-ray diffraction profile of Bi2O3 revealed the α-Bi2O3 monoclinic struc
J. Braz. Chem. Soc.. Publicado em: 2019-04
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10. CuO Rapid Synthesis with Different Morphologies by the Microwave Hydrothermal Method
CuO structures were synthesized by microwave hydrothermal treatment using two different mineralizing agents (NaOH and NH4OH) and were evaluated as photocatalysts. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and Brunauer-Emmett-Teller (BET) surface area analysis. The XRD patterns indicated the formation of
Mat. Res.. Publicado em: 11/10/2018
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11. Evaluation of the Sustainability of Integrated Hydrothermal Synthesis of Zeolites Obtained from Waste
The high Si and Al contents in the amorphous phase of coal fly ash have been used for its conversion into zeolites. This process converts a toxic low-value by-product into a product used in a number of environmental applications, but has the disadvantage of introducing contaminants. Despite the large number of studies on the conversion of fly ash into zeolit
J. Braz. Chem. Soc.. Publicado em: 2018-07
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12. Effect of Different Synthesis Methods on the Textural Properties of Calcium Tungstate (CaWO4) and Its Catalytic Properties in the Toluene Oxidation
Calcium tungstate (CaWO4) crystals were prepared by microwave-assisted hydrothermal (MAH) and polymeric precursor methods (PPM). These crystals were structurally characterized by X-ray diffraction (XRD), N2 adsorption, X-ray absorption near edge spectroscopy (XANES) and extended X-ray absorption fine structure (EXAFS) measurements. The morphology and size of
Mat. Res.. Publicado em: 16/04/2018