Electronic Microscopy
Mostrando 1-12 de 365 artigos, teses e dissertações.
-
1. EFFECT OF REACTION CONDITIONS ON PARTICLE SIZE OF ZNO NANOPARTICLES VIA CONTROLLED PRECIPITATION METHOD AND IN-VITRO ANTIBACTERIAL CAPACITY
High-yield ZnO spheroidal nanoparticles with an average diameter around 23 nm (≈ 25% frequency) and 30 nm (≈ 28% frequency) were obtained by controlled semicontinuous precipitation at low temperatures. This synthesis was obtained from hydrozincite (Zn5(CO3)2(OH)6) as primary nanoparticles. The Zn5(CO3)2(OH)6 nanoparticles were synthesized by hydrolysis o
Química Nova. Publicado em: 2022
-
2. Designing and fabrication of a low-cost dip-coater for rapid production of uniform thin films
In this work, a self-made dip-coater equipment was developed for the fabrication of thin films. The assembly of the apparatus was carried out using simple mechanical and electronic pieces, recycle parts, and spending an inexpensive budget suitably. The production, software design, and features of the device were focused on the sol-gel dip-coating method, whi
Química Nova. Publicado em: 2022
-
3. Dextran Sulfate/Pramlintide Polyelectrolyte Nanoparticles as a Promising Delivery System: Optimization, Evaluation of Supramolecular Interactions and Effect on Conformational Stability of the Peptide Drug
In this study, we investigated the feasibility to obtain nanoparticles (NPs) by assembling pramlintide (Pram) with dextran sulfate (DexS), as a new approach for mucosal peptide delivery. DexS/Pram NPs were prepared by dropwise addition of a Pram solution to a DexS solution under magnetic stirring. The physicochemical characteristics of NPs and molecular inte
J. Braz. Chem. Soc.. Publicado em: 2021-08
-
4. ERRATUM
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Arq. Neuro-Psiquiatr.. Publicado em: 2021-06
-
5. Polyamide 11 porous films by NIPS: the influence of miscibility and polymer crystalline formation in pores structure and morphology
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Quím. Nova. Publicado em: 2021-06
-
6. Heterotopic Heart Transplant History and Concepts Cannot Be Neglected - Witnessing the History and Learning with Previous Practices
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Braz. J. Cardiovasc. Surg.. Publicado em: 2021-06
-
7. Nickel-Cerium Layered Double Hydroxide as Electrocatalyst for Glycerol Oxidation
A new nickel based layered double hydroxide nanomaterial, Ni0.8Ce0.2-LDH, constituted by about 3 nm large nanoparticles exhibiting enhanced electrocatalytic properties towards oxidation of glycerol in alkaline media, was prepared by incorporation of 20 wt.% of CeIII ions into α-nickel hydroxide. This can be oxidized to CeIV, as demonstrated by X-ray photoel
J. Braz. Chem. Soc.. Publicado em: 2020-11
-
8. COVID-19 and stroke: a thromboembolic hypothesis
A new nickel based layered double hydroxide nanomaterial, Ni0.8Ce0.2-LDH, constituted by about 3 nm large nanoparticles exhibiting enhanced electrocatalytic properties towards oxidation of glycerol in alkaline media, was prepared by incorporation of 20 wt.% of CeIII ions into α-nickel hydroxide. This can be oxidized to CeIV, as demonstrated by X-ray photoel
Rev. Assoc. Med. Bras.. Publicado em: 2020-11
-
9. Calcium oxalate content from two Amazonian amilaceous roots and the functional properties of their isolated starches
Abstract The calcium oxalate content from two Amazonian amilaceous roots, Xanthosoma sagittifolium and Pachyrhizus tuberosus, before and after cooking were studied in the present work. Calcium oxalate raphides were observed by light microscopy in longitudinal sections from fresh tubers. The functional properties and physicochemical characteristics of isolate
Food Sci. Technol. Publicado em: 2020-09
-
10. Surface Silanization of Graphene Oxide Under Mild Reaction Conditions
The functionalization of graphene oxide with organosilanes is an important strategy to yield graphene-silica composites as well as to create nanomaterials for use as reinforcement in polymer nanocomposites and corrosion-inhibiting coatings for metals, among other uses. However, depending on the reaction conditions used, the organosilanes tend to self-condens
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
-
11. Effect of Solid Solution Temperature on Microstructure and Corrosion Resistance of CoNiCrMo Alloy
Influence of solid solution temperature on microstructures and corrosion properties of CoNiCrMo alloy were investigated by means of optical microscopy (OM), scanning electron microscope (SEM) and electronic differential system. The corrosion resistance of CoNiCrMo alloy in 0.9%NaCl aqueous solution was also investigated. The results indicated that with the i
Mat. Res.. Publicado em: 24/10/2019
-
12. Glass fiber post treatment – does it influence resin cement bond strength?
Resumo Introdução Pinos de fibra de vidro são utilizados para melhorar a retenção das restaurações em dentes tratados endodonticamente. Objetivo Avaliar a resistência de união de pinos de fibra de vidro submetidos a diferentes tratamentos superficiais e cimentados à dentina radicular com cimento resinoso autoadesivo. Material e método trinta ra
Rev. odontol. UNESP. Publicado em: 26/09/2019