Detectability
Mostrando 1-12 de 82 artigos, teses e dissertações.
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1. Rapid and Inexpensive Colorimetric Detection of Total Serum Protein Using Microzone Plates Wax-Printed on Polyester Films
This report describes a rapid and inexpensive colorimetric method based on biuret assay for total serum protein analysis using wax printed microzone plates and a desktop scanner. The colorimetric assay was performed in 96-microzone plates fabricated on polyester films through a wax printing protocol. The image scanning mode and the concentration of the biure
J. Braz. Chem. Soc.. Publicado em: 2021-02
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2. Detectability of Middle Mesial Canal in Mandibular Molar After Troughing Using Ultrasonics and Magnification: An Ex Vivo Study
Resumo O objetivo deste estudo foi avaliar a frequência de identificação do canal médio-mesial (MM) antes e após a execução da técnica de troughing sob ampliação microscópica em primeiros e segundos molares inferiores permanentes extraídos. A amostra foi composta por 105 molares inferiores. Após abertura coronária e limpeza do assoalho pulpar,
Braz. Dent. J.. Publicado em: 03/06/2019
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3. EXTRAÇÃO EM FASE SÓLIDA DE RESÍDUOS DE AGROTÓXICOS DE ÁGUA SUPERFICIAL, EMPREGANDO UM SORVENTE DE MENOR RETENÇÃO
Solid phase extraction (SPE) is one of the main sample preparation techniques. However, the cost of cartridges and the strong retention of hydrophobic compounds in traditional solid phases are limiting factors for their use. This paper describes the application of lab-made SPE cartridges with low retention material as solid phase, Si(PDAS) - poly(dimethyl-co
Quím. Nova. Publicado em: 2018-06
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4. Alkaline Solubilization of Chicken Tissues Monitored by Raman Spectroscopy Followed by Pb Determination by GF AAS
This paper proposes a method for chicken tissues preparation using tetramethylammonium hydroxide (TMAH) for Pb determination by graphite furnace atomic absorption spectrometry employing multivariate approaches. Combining Raman spectroscopy with scanning electron microscopy coupled to energy-dispersive X-ray spectroscopy to monitor the solubilization process
J. Braz. Chem. Soc.. Publicado em: 2018-02
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5. Solid-phase extractions in flow analysis
ABSTRACT Coupling solid-phase extraction (SPE) to flow systems has promoted a synergistic development. Whereas SPE mechanization leads to improved precision and higher sample throughput, as well as diminishes systematic errors and contamination risks, analyte concentration and separation from the sample matrix provides a remarkable impact on detectability an
An. Acad. Bras. Ciênc.. Publicado em: 2018
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6. Sinais de fundo em análise instrumental: uma discussão essencial em cursos de graduação
Understanding instrumental analysis is essential for obtaining reliable analytical results required by chemists in a variety of research areas and industrial activities. All instrumental techniques involve undesirable background (BG) signals originated either from concomitants in the sample or by spurious (e.g. electrical or optical) effects intrinsically re
Quím. Nova. Publicado em: 2017-02
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7. Evaluation of QuEChERS Sample Preparation and Gas Chromatography Coupled to Mass Spectrometry for the Determination of Pesticide Residues in Grapes
An effective analytical method for pesticides multiresidue determination in grape samples was developed and validated. A modified quick, easy, cheap, effective, robust and safe (QuEChERS) method was used to extract the target compounds. Several sorbent materials were tested for the clean-up step using dispersive solid phase extraction (d-SPE) and Florisil®
J. Braz. Chem. Soc.. Publicado em: 2016-09
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8. COMPARAÇÃO DE MÉTODOS POR CROMATOGRAFIA LÍQUIDA NA DETERMINAÇÃO DE MULTIRRESÍDUOS DE AGROTÓXICOS EM MORANGOS
Liquid chromatography is often used for the determination of pesticide multiresidues in foods. In Brazil, the strawberry crop is an example of a food with high levels of irregularities because of the application of pesticides. This is a major concern from the perspective of food safety, environmental protection, and certification for food export. The purpose
Quím. Nova. Publicado em: 2015-12
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9. New structures for goat corrals to control peridomestic populations of Triatoma infestans (Hemiptera: Reduviidae) in the Gran Chaco of Argentina
Goat production is an important economic activity for rural communities in the Gran Chaco of Argentina. Goat corrals are important for the survival of peridomestic populations of Triatoma infestans. This study evaluated the impact of modifying the traditional structure of goat corrals on T. infestans populations and goat productivity in the region of Los Ll
Mem. Inst. Oswaldo Cruz. Publicado em: 2013-05
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10. Aspectos analíticos e regulatórios na determinação de resíduos de macrolídeos em alimentos de origem animal por cromatografia líquida associada à espectrometria de massas
This is an overview of LC-MS techniques applied for macrolide determination in food, including sample preparation and method validation, as well as the policies adopted by international agencies regarding their presence in food. Techniques for the analysis of macrolides in food normally include solid phase or liquid-liquid extraction followed by HPLC. UHPLC
Quím. Nova. Publicado em: 2013
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11. A weight restricted DEA model for FMEA risk prioritization
In this paper we present a linear programming (LP) approach to risk prioritization in failure mode and effects analysis (FMEA). The LP is a data envelopment analysis (DEA)-based model considering weight restriction. In a FMEA, we commonly consider three criteria to prioritize the failure modes, occurrence, severity and detectability. These criteria are in an
Prod.. Publicado em: 22/11/2012
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12. Desenvolvimento de métodos cromatográficos hifenados (in-tube SPME/LC-FLD e GCxGC/qMS) para análises de fármacos e agrotóxicos em amostras complexas / Development of hyphenated chromatographic methods (in-tube SPME/LC-FLD and GCxGC/MS) for analysis of drugs and pesticides in complex samples.
Determination of trace levels of drugs in biological fluids and multiresidue (contaminants) in food samples is extremely important because this generates valuable data for therapeutic drug monitoring (individualization of dosage regimen) and quality control (food safety), respectively. Because of the demand for analytical methods with high resolution and low
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 25/07/2011